Mass spectrometric analysis of black market products by HPLC-(HR)MS, GC-(HR)MS and 1D-gel electrophoresis-UPLC-MSn
| Deutscher übersetzter Titel: | Massenspektrometrische Analyse von Schwarzmarktprodukten mittels HPLC-(HR)MS, GC-(HR)MS und 1D-gel Elektrophorese-UPLC-MSn |
|---|---|
| Autor: | Krug, Oliver; Thomas, Andreas; Walpurgis, Katja; Piper, Thomas; Sigmund, Gerd; Geyer, Hans; Schänzer, Wilhelm; Thevis, Mario |
| Erschienen in: | Recent advances in doping analysis (21) : Proceedings of the Manfred-Donike-Workshop ; 31th Cologne Workshop on Dope Analysis ; 24th February to 1st March 2013 |
| Veröffentlicht: | Köln: Sportverl. Strauß (Verlag), 2013, S. 169-172, Lit. |
| Format: | Literatur (SPOLIT) |
| Publikationstyp: | Sammelwerksbeitrag |
| Medienart: | Elektronische Ressource (Datenträger) |
| Sprache: | Englisch |
| Schlagworte: | |
| Online Zugang: | |
| Erfassungsnummer: | PU201408007441 |
| Quelle: | BISp |
Abstract
In order to prevent deception by abuse of drugs in sport terms and its health-risk, the World-Anti-Doping-Agency (WADA) publishes the annually updated Prohibited List. Not only top athletes, but also the athletes of mass sport succumb the abuse of performing enhancing agents. In total 185 black market products as well as products confiscated by the police or the bureau of customs investigation were analysed qualitatively and quantitatively since 2010. The samples contained 38 different drugs with doping relevancy and in most cases unlabeled drugs could be confirmed. An outstanding result was the identification of methyltestosterone in 21 samples, which contained up to 112 mg/mL. Furthermore the steroidal derivatives 5α-androstano-(2,3-c)-furazan-17β-tetrahydropyranol and 17-methyl-stenbolone were identified. Verf.-Referat